HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → HCID 67153333, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | Formic Acid | HCID 284 | — |
| Reactant | HCID 58277334 | HCID 58277334 | — |
| Reactant | HCID 67153505 | HCID 67153505 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 67153333 | HCID 67153333 | — |
Reaction Steps
The preparation of the title compound takes place starting from the compound of Example 120A and a 7N solution of ammonia in methanol with the addition of 0.1% formic acid in the preparative HPLC in analogy to the synthesis of the compound of Example 29. 10 mg (10% of theory) of the title compound are obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08399682B2 |
| Source dataset | uspto-grants-2013_03 |
| ORD ID | ord-e7533b44bfac43c6b60b5a574d4d8e86 |
| Source note | uspto-grants-2013_03 |