HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diisopropylethylamine → HCID 44230248, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diisopropylethylamine | HCID 81531 | — |
| Reactant | HCID 58277296 | HCID 58277296 | — |
| Reactant | HCID 58277360 | HCID 58277360 | — |
| Solvent | Formic Acid | HCID 284 | — |
| Product | HCID 44230248 | HCID 44230248 | — |
Reaction Steps
The preparation of the title compound takes place starting from the compound of Example 111A using 3.2 equivalents of N,N-diisopropylethylamine and with the addition of 0.1% formic acid in the preparative HPLC in analogy to the synthesis of the compound of Example 23. 16 mg (29% of theory) of the title compound are obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08399682B2 |
| Source dataset | uspto-grants-2013_03 |
| ORD ID | ord-04ea1f1cf5d14287acc437040eb8f401 |
| Source note | uspto-grants-2013_03 |