HRID1949502

反应详情

EQUATION

反应方程式

HRID 1949502 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

To a solution of 2-methylsulfanyl-thiazol-4-one (4.4 g, 30 mmol) in MeOH (60 mL) was added piperidine-4-carboxylic acid (3.9 g, 30 mmol). The mixture was stirred at room temperature for 16 hours. The resulting solid was collected by filtration and washed with fresh MeOH.

WORKUP

后处理

  1. filtrationThe resulting solid was collected by filtration
  2. washwashed with fresh MeOH