HuagongsheHuagongshe Chemistry Print Report · For research reference only
6-Methoxy-3,4-dihydronaphthalen-2-yl trifluoromethanesulfonate → 7-Methoxy-3-(4-methoxy-2-nitrophenyl)-1,2-dihydronaphthalene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 6-Methoxy-3,4-dihydronaphthalen-2-yl trifluoromethanesulfonate | HCID 15330256 | — |
| Reactant | Tributyl(4-methoxy-2-nitrophenyl)tin | HCID 23087474 | — |
| Product | 7-Methoxy-3-(4-methoxy-2-nitrophenyl)-1,2-dihydronaphthalene | HCID 23087141 | 73.2% |
Reaction Steps
Synthesized from 6-methoxy-3,4-dihydronaphthalen-2-yl trifluoromethanesulfonate (2.3 g) and tributyl(4-methoxy-2-nitrophenyl)tin (3.9 g) according to an analogous synthetic method to Preparation Example 77, the title compound (1.7 g) was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08399520B2 |
| Source dataset | uspto-grants-2013_03 |
| ORD ID | ord-abad95a7466a44ad9de9febe7ddd41a6 |
| Source note | uspto-grants-2013_03 |