HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,3-Dimethoxybenzene → 1-(2,4-Dimethoxyphenyl)-2-(4-methoxyphenyl)ethanone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,3-Dimethoxybenzene | HCID 9025 | — |
| Reactant | 4-Methoxyphenylacetyl chloride | HCID 2734688 | — |
| Product | 1-(2,4-Dimethoxyphenyl)-2-(4-methoxyphenyl)ethanone | HCID 13427163 | 51.6% |
Reaction Steps
Synthesized from 1,3-dimethoxybenzene (8.2 g) and 4-methoxyphenylacetyl chloride (10.0 g) according to an analogous synthetic method to Preparation Example 66, the title compound (8.0 g) was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08399520B2 |
| Source dataset | uspto-grants-2013_03 |
| ORD ID | ord-7c4ec359f6f74e8c98cad45bbe85a692 |
| Source note | uspto-grants-2013_03 |