HuagongsheHuagongshe Chemistry Print Report · For research reference only
Carbon tetrabromide → 6-Bromo-pentadecane
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Carbon tetrabromide | HCID 11205 | — |
| Reactant | Triphenylphosphine | HCID 11776 | — |
| Reactant | 6-Pentadecanol | HCID 98974 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | 6-Bromo-pentadecane | HCID 86639780 | 86% |
Reaction Steps
The title compound (13.87 g) was prepared from Pentadecan-6-ol (Example 11, 12.65 g), carbon tetrabromide (22 g), triphenylphosphine (24.82 g) and dichloromethane (200 ml) using the procedure of Example 6.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08404627B2 |
| Source dataset | uspto-grants-2013_03 |
| ORD ID | ord-ea44599a986743be86af6014eb357e0f |
| Source note | uspto-grants-2013_03 |