HuagongsheHuagongshe Chemistry Print Report · For research reference only
Salicylic Acid → HCID 140546754, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Salicylic Acid | HCID 338 | — |
| Reactant | O-Xylene | HCID 7237 | — |
| Reactant | Calcium Hydroxide | HCID 6093208 | — |
| Reactant | HCID 68551883 | HCID 68551883 | — |
| Solvent | Methanol | HCID 887 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 140546754 | HCID 140546754 | — |
Reaction Steps
The title compound in 4 g of base oil XOMAPE 150 (13.2 g, Basicity Index 1.48) was prepared as outlined in Example 4 by employing 5-(pentadecy-6-yl)salicylic acid (Example 15, 3.3 g), a commercial lower alkyl (i.e. less than C20) salicylic acid (Infineum M7103, obtainable from Infineum UK Limited, 3.70 g), xylene (203 g), calcium hydroxide (4 g), and a promoter (methanol:water (97%:3%), 23.4 ml).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08404627B2 |
| Source dataset | uspto-grants-2013_03 |
| ORD ID | ord-5de8201cd4654d468eb5be8d406ed0f4 |
| Source note | uspto-grants-2013_03 |