HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Methylmorpholine → HCID 86761782, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Methylmorpholine | HCID 7972 | — |
| Reactant | PyBOP | HCID 2724699 | — |
| Product | HCID 86761782 | HCID 86761782 | — |
Reaction Steps
To the resin were added Fmoc-amino acid (6 equiv, 0.6 M in NMP), PyBOP (6 equiv, 0.67 M in NMP) and NMM (12 equiv, 33% solution in NMP). The coupling reaction was performed for 90 min with occasional shaking and at the end of the coupling the resin was washed with NMP (6×0.8 ml).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08404647B2 |
| Source dataset | uspto-grants-2013_03 |
| ORD ID | ord-9c3f1fbbacf4489084d375ab92a7d76e |
| Source note | uspto-grants-2013_03 |