Hydrochloric Acid → HCID 67426793, compound

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To a solution of 1-(2-(tert-butoxycarbonyl)-methylamino-ethoxy)-3,5-bis-(tert-butyl-dimethyl-silyloxy methyl)-benzene (590 mg) in dioxane (4 mL) was added a solution of hydrochloric acid 4N in dioxane (3.3 mL). After 15 h at rt, the resulting solid was filtered, washed with dioxane and dried in vacuo to give 3,5-bis-hydroxymethyl-(2-methylamino-ethoxy)-benzene hydrochloride (240 mg) as a white powder. LC/MS (Method A2): ES: m/z 212 (M+H)+; RT=0.14 min

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