HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylformamide dimethyl acetal → HCID 58494269, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylformamide dimethyl acetal | HCID 78373 | — |
| Reactant | HCID 58494233 | HCID 58494233 | — |
| Product | HCID 58494269 | HCID 58494269 | — |
Reaction Steps
The title compound was prepared as described in Example 1e by starting from ethyl 4-methyl-2-(methylthio)-6-(3-(trifluoromethyl)phenylamino)pyrimidine-5-carboxylate 1.76 g (4.74 mmol) and N,N-dimethyl formamide dimethylacetal (947 uL, 7.1 mmol) and continuing until the reaction yielded the crude title compound. This was used for the next step without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08404677B2 |
| Source dataset | uspto-grants-2013_03 |
| ORD ID | ord-99e4aa3ef207459b8b0cceb7bb2408c9 |
| Source note | uspto-grants-2013_03 |