HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonium Hydroxide → HCID 86658934, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonium Hydroxide | HCID 14923 | — |
| Reactant | HCID 86658935 | HCID 86658935 | — |
| Product | HCID 86658934 | HCID 86658934 | — |
Reaction Steps
The title compound was prepared as described in Example 1f by starting from (E)-ethyl 4-(3,5-bis(trifluoromethyl)phenylamino)-6-(2-(dimethylamino)vinyl)-2-(methylthio)pyrimidine-5-carboxylate and aq. NH4OH solution and continuing until the reaction yielded pale yellow solids, title compound (537 mg). MS m/z: 421.1 (M+1)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08404677B2 |
| Source dataset | uspto-grants-2013_03 |
| ORD ID | ord-d0f01aa0355540a39840999dd45fc6e7 |
| Source note | uspto-grants-2013_03 |