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HRID1950787

反应详情

EQUATION

反应方程式

HRID 1950787 的结构方程式

REACTANTS

反应物

2
结构：[NH4+].[OH-]
HCID14923

Ammonium hydroxide

H5NO

结构：CCOC(=O)c1c(/C=C/N(C)C)nc(SC)nc1Nc1cc(C(F)(F)F)cc(C(F)(F)F)c1
HCID86658935

未命名化合物

PRODUCTS

生成物

1
结构：CSc1nc(Nc2cc(C(F)(F)F)cc(C(F)(F)F)c2)c2c(=O)[nH]ccc2n1
HCID86658934

未命名化合物

PROCEDURE

实验过程

The title compound was prepared as described in Example 1f by starting from (E)-ethyl 4-(3,5-bis(trifluoromethyl)phenylamino)-6-(2-(dimethylamino)vinyl)-2-(methylthio)pyrimidine-5-carboxylate and aq. NH4OH solution and continuing until the reaction yielded pale yellow solids, title compound (537 mg). MS m/z: 421.1 (M+1)+.

WORKUP

后处理

  1. customThe title compound was prepared