HuagongsheHuagongshe Chemistry Print Report · For research reference only
Piperidin-4-ol → HCID 58494270, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Piperidin-4-ol | HCID 79341 | — |
| Reactant | HCID 58494211 | HCID 58494211 | — |
| Product | HCID 58494270 | HCID 58494270 | 60% |
Reaction Steps
The title compound was prepared as described in Example 1g by starting from 8-bromo-2-(methylthio)-4-(3-(trifluoromethyl)phenylamino)pyrido[4,3-d]pyrimidin-5(6H)-one (60 mg, 0.26 mmol) and 4-hydroxypiperidine and continuing until the reaction yielded the title compound (40 mg, 60%)) as grey solid. MS m/z: 484 and 486 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08404677B2 |
| Source dataset | uspto-grants-2013_03 |
| ORD ID | ord-f81a76e25e4844bba5e2731fdfc28352 |
| Source note | uspto-grants-2013_03 |