Triethylamine → HCID 59185808, compound

Participants

Reaction Steps

4-Acetyl-3,5-dimethyl-1H-pyrrole-2-carboxylic acid (2-chloro-ethyl)-amide (12.664 g, 52.18 mmol) was slurried in DCM (100 mL) and Et3N (20 mL) and heated to 50° C. for 16 hours. After cooling to room temperature and removal of solvent, the residue was treated with cold water. The resulting off white precipitate filtered off and shown to be the target compound (10.424 g, 50.54 mmol, 97% yield).

Provenance & Evidence