HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 46205404, compound → HCID 46205728, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 46205404 | HCID 46205404 | — |
| Solvent | Carbon Tetrachloride | HCID 5943 | — |
| Product | HCID 46205728 | HCID 46205728 | — |
Reaction Steps
From 2d (yield: 83%) as an oil; IR (CCl4) 2956, 1550, 1253 cm−1; 1H NMR (400 MHz, CDCl3) δ 3.89 (s, 3H), 5.05 (s, 2H), 6.74 (t, 1H, J=7 Hz), 6.89 (dd, 1H, J=2.5, 8 Hz), 7.06 (d, 1H, J=7 Hz), 7.34 (t, 1H, J=8 Hz), 7.51 (d, 1H, J=8 Hz), 7.54 (d, 1H, J=2.5 Hz), 7.83 (s, 1H), 8.03 (d, 1H, J=7 Hz); 13C NMR (100 MHz, CDCl3) δ 55.4, 62.6, 108.4, 111.4, 112.4, 113.9, 118.6, 121.4, 124.6, 129.7, 129.8, 134.9, 144.6, 144.9, 160.0; MS m/z 254 (M+, 58), 253 (100), 238 (12), 225 (22), 210 (16).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08404707B2 |
| Source dataset | uspto-grants-2013_03 |
| ORD ID | ord-ed3d8fda9e4b48cbb4dce4d03fe15297 |
| Source note | uspto-grants-2013_03 |