HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 46205727, compound → HCID 46205731, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 46205727 | HCID 46205727 | — |
| Solvent | Carbon Tetrachloride | HCID 5943 | — |
| Product | HCID 46205731 | HCID 46205731 | — |
Reaction Steps
From 2g (yield: 52%) as an oil; IR (CCl4) 2962, 1498 cm−1; 1H NMR (400 MHz, CDCl3) δ 1.09 (s, 9H), 4.72 (s, 2H), 5.01 (s, 1H), 6.39 (t, 1H, J=7 Hz), 6.73 (d, 1H, J=7 Hz), 7.03 (s, 1H), 7.67 (d, 1H, J=7 Hz); 13C NMR (100 MHz, CDCl3) δ 30.1, 32.2, 62.4, 106.8, 111.6, 124.4, 129.1, 143.9, 156.4; MS m/z 204 (M+, 53), 203 (100), 175 (24), 171 (55).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08404707B2 |
| Source dataset | uspto-grants-2013_03 |
| ORD ID | ord-46da9df358d149eeba1f3bb1924e7f4a |
| Source note | uspto-grants-2013_03 |