HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Bromide → HCID 46205398, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Bromide | HCID 253877 | — |
| Reactant | HCID 46205077 | HCID 46205077 | — |
| Product | HCID 46205398 | HCID 46205398 | — |
Reaction Steps
From 2i (yield: 60%); mp 87-89° C.; IR (KBr) 2977, 1148 cm−1; 1H NMR (400 MHz, CDCl3) δ 1.25 (t, 6H, J=7 Hz), 3.68 (m, 4H), 4.52 (brs, 1H), 5.02 (s, 2H), 5.71 (s, 1H), 6.75 (t, 1H, J=7 Hz), 7.12 (d, 1H, J=7 Hz), 7.65 (s, 1H), 8.00 (d, 1H, J=7 Hz); 13C NMR (100 MHz, CDCl3) δ 15.3, 61.7, 61.9, 98.6, 106.1, 110.7, 112.5, 121.5, 124.8, 130.2, 143.9; MS m/z 250 (M+, 4), 206 (33), 177 (100), 175 (38), 159 (91), 78 (15).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08404707B2 |
| Source dataset | uspto-grants-2013_03 |
| ORD ID | ord-18fb4bfd20d2455c884d2d61672f5bdc |
| Source note | uspto-grants-2013_03 |