HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 46205398, compound → HCID 46205399, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 46205398 | HCID 46205398 | — |
| Solvent | Carbon Tetrachloride | HCID 5943 | — |
| Product | HCID 46205399 | HCID 46205399 | 98% |
Reaction Steps
From 3i: reaction time 15 h (yield: 98%) as an oil; IR (CCl4) 1693, 1056 cm−1; 1H NMR (400 MHz, CDCl3) δ 1.30 (t, 6H, J=7 Hz), 3.73 (m, 4H), 5.79 (s, 1H), 6.96 (t, 1H, J=7 Hz), 7.80 (s, 1H), 7.83 (d, 1H, J=7 Hz), 8.34 (d, 1H, J=7 Hz), 10.82 (s, 1H); 13C NMR (100 MHz, CDCl3) δ 15.3, 62.0, 98.6, 111.0, 112.0, 124.1, 125.7, 130.6, 144.1, 146.8, 189.1; MS m/z 248 (M+, 1), 204 (17), 175 (100).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08404707B2 |
| Source dataset | uspto-grants-2013_03 |
| ORD ID | ord-d6018fb261394d0d94d95a31e3b7b1bb |
| Source note | uspto-grants-2013_03 |