Potassium Bromide → HCID 67360692, compound

Participants

Reaction Steps

From 25c (yield: 55%); mp 162° C.; IR (KBr) 3061, 2924, 1637, 1528 cm−1; 1H NMR (400 MHz, CDCl3) δ 0.82 (t, 3H, J=7.6 Hz), 1.28 (m, 2H), 1.60 (m, 2H), 2.43 (s, 3H), 2.69 (t, 2H, J=7.6 Hz), 6.56 (s, 1H), 6.82 (d, 1H, J=7.1 Hz), 7.20 (s, 1H), 7.62 (d, 1H, J=7.1 Hz), 10.37 (s, 1H); 13C NMR (100 MHz, CDCl3) δ 13.8, 14.2, 22.3, 27.8, 31.5, 98.8, 101.2, 108.9, 114.1, 118.8, 130.4, 139.1, 139.8, 142.0. Anal. Calcd for C14H17N3: C, 73.98; H, 7.54; N, 18.49. Found: C, 74.05; H, 7.51; N, 18.29.

Provenance & Evidence