Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 45377063 | HCID 45377063 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 45377209 | HCID 45377209 | 169.8% |
Reaction Steps
The product (0.86 grams) obtained from Example 1 was converted into its hydrochloride salt by using the following procedure. The obtained base was taken into diethyl ether (25 mL) and added 1 mL of 10% isopropanolic hydrogen chloride. The reaction mass was stirred for 3 hours at 25-30° C. and filtered the hydrochloride salt to obtain the title product (0.8 grams).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US08404720B2 |
|---|
| Source dataset | uspto-grants-2013_03 |
|---|
| ORD ID | ord-4d64d20eb3784378b275e1c5a86da2f5 |
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| Source note | uspto-grants-2013_03 |
|---|
