Benzylamine → HCID 11043015, compound

Participants

Reaction Steps

4 Å molecular sieve (20 g) and benzylamine (8.90 g, 83 mmol) were added to a solution of 1,4-dioxaspiro[4.5]decan-8-one (10.0 g, 64 mmol) in dichloromethane (100 ml), and the reaction mixture was stirred for 16 h at room temperature. The suspension was then filtered and the filtrate was concentrated in vacuo.

Provenance & Evidence