1,4-Dioxane hydrochloride → HCID 67426079, compound

Participants

Reaction Steps

4 N hydrochloric acid/dioxane (8 ml) was added to a dioxane (10 ml) solution of the compound (0.57 g, 1.42 mmol) obtained in Step 4 above under ice cooling and the resulting mixture was gradually returned to room temperature while being stirred for 24 hours. The reaction mixture was concentrated under reduced pressure to give the title compound as a colorless solid.

Provenance & Evidence