HuagongsheHuagongshe Chemistry Print Report · For research reference only
6,6-Dimethyl-1-Vinylcyclohexene → HCID 68601845, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 6,6-Dimethyl-1-Vinylcyclohexene | HCID 11829503 | — |
| Reactant | 2-[(Prop-2-en-1-yl)oxy]cyclohexa-2,5-diene-1,4-dione | HCID 46911800 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 68601845 | HCID 68601845 | 36% |
Reaction Steps
2-Allyloxy-1,4-benzoquinone (10.0 g, 60.9 mM) and 6,6-Dimethyl-1-Vinylcyclohexene (19.8 g, 183 mM) were dissolved in 100 ml of MeOH, and refluxed for 3 hours. 3-Allyloxy-8,8-dimethyl-5,6,7,8-tetrahydro-1,4-phenanthrenequinone (6.5 g, 22.0 mM) was obtained in the same manner as in Example 1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08404869B2 |
| Source dataset | uspto-grants-2013_03 |
| ORD ID | ord-4aabd890050f4c0b8708cb28deb74d13 |
| Source note | uspto-grants-2013_03 |