huagongshe.com
HRID1952274

反应详情

EQUATION

反应方程式

HRID 1952274 的结构方程式

REACTANTS

反应物

2
反应SMILES：C=CC1=CCCCC1
HCID17497

1-Vinylcyclohexene

C8H12

反应SMILES：CC(C)=CCOC1=CC(=O)C=CC1=O
HCID53420490

2,5-Cyclohexadiene-1,4-dione, 2-[(3-methyl-2-buten-1-yl)oxy]-

C11H12O3

PRODUCTS

产物

1
反应SMILES：CC(C)=CCOC1=CC(=O)c2ccc3c(c2C1=O)CCCC3
HCID68600744

未命名化合物

收率 34.8%

AUXILIARIES

试剂、催化剂与溶剂

1
反应SMILES：CO
溶剂HCID887

Methanol

CH4O

PROCEDURE

实验过程

2-Prenyloxy-1,4-benzoquinone (3.0 g, 15.6 mM) and 1-Vinylcyclohexene (6.75 g, 62.5 mM) were dissolved in 50 ml of MeOH, and refluxed for 3 hours. 3-Prenyloxy-5,6,7,8-tetrahydro-1,4-phenanthrenequinone (1.61 g, 5.44 mM) was obtained in the same manner as in Example 1.

WORKUP

后处理

  1. temperaturerefluxed for 3 hours