HuagongsheHuagongshe Chemistry Print Report · For research reference only
Vinylcyclohexene → HCID 68600744, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Vinylcyclohexene | HCID 17497 | — |
| Reactant | 2,5-Cyclohexadiene-1,4-dione, 2-[(3-methyl-2-buten-1-yl)oxy]- | HCID 53420490 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 68600744 | HCID 68600744 | 34.8% |
Reaction Steps
2-Prenyloxy-1,4-benzoquinone (3.0 g, 15.6 mM) and 1-Vinylcyclohexene (6.75 g, 62.5 mM) were dissolved in 50 ml of MeOH, and refluxed for 3 hours. 3-Prenyloxy-5,6,7,8-tetrahydro-1,4-phenanthrenequinone (1.61 g, 5.44 mM) was obtained in the same manner as in Example 1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08404869B2 |
| Source dataset | uspto-grants-2013_03 |
| ORD ID | ord-1a65e1b4bd5a4cd6927492f51e8c2072 |
| Source note | uspto-grants-2013_03 |