HuagongsheHuagongshe Chemistry Print Report · For research reference only
6,6-Dimethyl-1-Vinylcyclohexene → HCID 68599654, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 6,6-Dimethyl-1-Vinylcyclohexene | HCID 11829503 | — |
| Reactant | 2,5-Cyclohexadiene-1,4-dione, 2-[(3-methyl-2-buten-1-yl)oxy]- | HCID 53420490 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 68599654 | HCID 68599654 | 35.5% |
Reaction Steps
2-Prenyloxy-1,4-benzoquinone (20.0 g, 0.104 M) and 6,6-Dimethyl-1-vinylcyclohexene (56.7 g, 0.416 M) were dissolved in 150 ml of MeOH, and refluxed for 3 hours. 3-Prenyloxy-8,8-dimethyl-5,6,7,8-tetrahydro-1,4-phenanthrenequinone (12.0 g, 0.037 M) was obtained in the same manner as in Example 1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08404869B2 |
| Source dataset | uspto-grants-2013_03 |
| ORD ID | ord-bb179e931187487da5ddf342071d15f0 |
| Source note | uspto-grants-2013_03 |