HCID 57702307, compound → HCID 57702302, compound

Participants

Reaction Steps

A solution of 1,2-epithio-3-hexyl-3-butene (40 mg, 0.24 miol) and Cu(hfacac)2 (1.2 mg, 2.4 μmol) in benzene (1 mL) was heated at 100° C. for 1 h in a pressure tube. Concentration of the solvent in vacuo afforded a residue, which was purified by column chromatography (n-pentane) to give 3-Hexyl-2,5-dihydrothiophene (38 mg, 95%) as a colorless oil.

Provenance & Evidence