HCID 178418361, compound → HCID 178510691, compound

Participants

Reaction Steps

A mixture of 286 mg (1.64 mmol) of 1-2 and 35 mg of 10% palladium on carbon catalyst in 2 mL of absolute EtOH was hydrogentated at 1 atmosphere pressure using a hydrogen filled balloon. After approximately 2 hours, the reaction was determined to be complete by LC-MS analysis. The reaction was filtered through a Celite pad, and the filtrate concentrated in vacuo to give the title product as a pale yellow oil. MS M+1=149.

Provenance & Evidence