HCID 59529775, compound → HCID 178509912, compound

Participants

Reaction Steps

In a manner identical to that described above in Step 6 for Compound 3-8, from Compound 3-7 (325 mg; 0.604 mmol) was collected Compound 3-8 and the title compound 3-9 as a by product. MS M+1=391.8: 1H NMR (DMSO-d6): 2.90 (m, 2H), 3.20 (m, 2H), 5.75 (s, 1H), 7.12 (m, 1H), 7.20 (m, 1H), 7.55 (m, 1H), 7.64 (m, 2H), 8.20 (m, 1H), 8.45 (m, 1H), 12.30 (s, 1H), 13.25 (s, 1H).

Provenance & Evidence