Diethylamine → HCID 178464498, compound

Participants

Reaction Conditions

Reaction Steps

Phenyldichlorophosphine (4.47 g, 25.0 mmol) was dissolved in 80 mL of toluene and then cooled to 0° C. under N2. Diethylamine (3.65 g, 50.0 mmol) was added dropwise and the resulting reaction mixture was allowed to warm-up to room temperature (ca. 20° C.) overnight (ca. 12 hrs). Reaction was then filtered and the liquid phase was concentrated to give 5.25 g (97% yield) of N,N-diethyl-phenylphosphoramidous chloride.

Provenance & Evidence