HuagongsheHuagongshe Chemistry Print Report · For research reference only
Lawesson's reagent → HCID 23300105, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Lawesson's reagent | HCID 87949 | — |
| Reactant | HCID 11022747 | HCID 11022747 | — |
| Product | HCID 23300105 | HCID 23300105 | — |
Reaction Steps
150 mg (0.51 mmol) of isopropyl 6-chloro-3-ethylquinolin-2(1H)-one-4-carboxylate (Example 10) are reacted with Lawesson's reagent according to the process described in Example 5 (reaction time 5 hours at reflux temperature) and purified by means of chromatography on silica gel as indicated above (mobile phase: n-heptane/ethyl acetate=2/1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06114349 |
| Source dataset | uspto-grants-2000_09 |
| ORD ID | ord-dd9ba43464c344538ac79e087e13e479 |
| Source note | uspto-grants-2000_09 |