HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 88177687, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Ethanol | HCID 702 | — |
| Reactant | HCID 53763132 | HCID 53763132 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 88177687 | HCID 88177687 | — |
Reaction Steps
4N Hydrochloric acid--ethyl acetate solution (0.19 ml) was added to a solution of [2-[[N-[3-(dimethylamino)propyl]carbamoyloxy]methyl]phenyl]-N-octadecylformamide (0.20 g) in ethyl acetate (4 ml) while being cooled with ice. After being stirred for 10 minutes, the deposited crystals were dissolved with ethanol and the solution was concentrated. The residue was recrystallized from ethyl acetate, thereby yielding 0.21 g of the aimed compound as white crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06114325 |
| Source dataset | uspto-grants-2000_09 |
| ORD ID | ord-d2b7441224ed4d75840fcf63bcb8e76d |
| Source note | uspto-grants-2000_09 |