HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 23299376, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 23299377 | HCID 23299377 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 23299376 | HCID 23299376 | — |
Reaction Steps
4N Hydrochloric acid--ethyl acetate solution (0.12 ml) was added to a solution of [2-[[N-[3-(dimethylamino)propyl]carbamoyloxy]methyl]phenyl]-N-tetradecylformamide (0.200 g) in ethyl acetate (2 ml) at room temperature. After being stirred for 15 minutes, the reaction mixture was concentrated. The residue was recrystallized from ethyl acetate, thereby yielding 0.197 g of the aimed compound as white crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06114325 |
| Source dataset | uspto-grants-2000_09 |
| ORD ID | ord-b533e3648ae947729ec82ccb6edc91a9 |
| Source note | uspto-grants-2000_09 |