Hydrochloric Acid → HCID 23299376, compound

HRID 1952796Notes

Reaction equation

HRID 1952796 reaction equation
[ClH:1].[CH3:2][N:3]([CH3:35])[CH2:4][CH2:5][CH2:6][NH:7][C:8]([O:10][CH2:11][C:12]1[CH:17]=[CH:16][CH:15]=[CH:14][C:13]=1[N:18]([CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][CH2:27][CH2:28][CH2:29][CH2:30][CH2:31][CH2:32][CH2:33][CH3:34])[CH:19]=[O:20])=[O:9]>C(OCC)(=O)C>[ClH:1].[CH3:35][N:3]([CH3:2])[CH2:4][CH2:5][CH2:6][NH:7][C:8]([O:10][CH2:11][C:12]1[CH:17]=[CH:16][CH:15]=[CH:14][C:13]=1[N:18]([CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][CH2:27][CH2:28][CH2:29][CH2:30][CH2:31][CH2:32][CH2:33][CH3:34])[CH:19]=[O:20])=[O:9]

Participants

4

Reactant 2

HCID 313Hydrochloric AcidHCID 23299377HCID 23299377, compound

Product 1

HCID 23299376HCID 23299376, compound

Reagents, catalysts & solvents 1

HCID 8857Ethyl AcetateSolvent2×

Procedure

4N Hydrochloric acid--ethyl acetate solution (0.12 ml) was added to a solution of [2-[[N-[3-(dimethylamino)propyl]carbamoyloxy]methyl]phenyl]-N-tetradecylformamide (0.200 g) in ethyl acetate (2 ml) at room temperature. After being stirred for 15 minutes, the reaction mixture was concentrated. The residue was recrystallized from ethyl acetate, thereby yielding 0.197 g of the aimed compound as white crystals.

Workup

  1. concentrationthe reaction mixture was concentrated
  2. customThe residue was recrystallized from ethyl acetate

Sources & evidence

ORD record
ord-b533e3648ae947729ec82ccb6edc91a9
Source dataset
uspto-grants-2000_09
Patent number
US06114325

Reaction notes

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