HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 88178182, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 53918373 | HCID 53918373 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 88178182 | HCID 88178182 | — |
Reaction Steps
4N Hydrochloric acid--ethyl acetate solution (0.26 ml) was added to a solution of [2-[[N-(3-morpholinopropyl)carbamoyloxy]methyl]phenyl]-N-octadecylformamide (0.30 g) in ethyl acetate (4 ml) at room temperature. After being stirred for 10 minutes, the reaction mixture was concentrated. The residue was recrystallized from ethyl acetate-ethanol mixed solvent, thereby yielding 0.27 g of the aimed compound as white crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06114325 |
| Source dataset | uspto-grants-2000_09 |
| ORD ID | ord-9201291041e94bb0aa47f1192a7a0969 |
| Source note | uspto-grants-2000_09 |