Hydrogen chloride-ethyl acetate → HCID 88176606, compound

Participants

Reaction Steps

4N Hydrochloric acid - ethyl acetate solution (0.12 ml) was added to a solution of [2-[[N-[2-(dimethylamino)ethyl]carbamoyloxy]methyl]phenyl]-N-octadecylformamide (0.200 g) in ethyl acetate (2 ml) at room temperature. After being stirred for 15 minutes, the reaction mixture was concentrated. The residue was recrystallized from ethyl acetate-ethanol mixed solvent, thereby yielding 0.205 g of the aimed compound as white crystals.

Provenance & Evidence