HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 88176610, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Ethyl Acetate | HCID 8857 | — |
| Reactant | HCID 54068388 | HCID 54068388 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 88176610 | HCID 88176610 | — |
Reaction Steps
4N Hydrochloric acid--ethyl acetate solution (0.10 ml) was added to a solution of [2-[[N-[3-(1-imidazolyl)propyl]carbamoyloxy]methyl]phenyl]-N-octadecylformamide (0.200 g) in ethanol (2 ml) at room temperature. After being stirred for 20 minutes, the reaction mixture was concentrated. The residue was recrystallized from ethyl acetate-ethanol mixed solvent, thereby yielding 0.201 g of the aimed compound as white crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06114325 |
| Source dataset | uspto-grants-2000_09 |
| ORD ID | ord-6f2cba8d948e4aeea1e75f0f6945929f |
| Source note | uspto-grants-2000_09 |