Hydrochloric Acid → HCID 88177700, compound

Participants

Reaction Steps

4N Hydrochloric acid--ethyl acetate solution (0.11 ml) was added to a solution of [2-[[N-(dimethylamino)carbamoyloxy]methyl]phenyl]-N-octadecylformamide (0.200 g) in ethyl acetate (6 ml) while being cooled with ice. After being stirred for 30 minutes at room temperature, the reaction mixture was concentrated. The residue was recrystallized from ethyl acetate-ethanol mixed solvent, thereby yielding 0.195 g of the aimed compound as white crystals.

Provenance & Evidence