HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 88176874, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 56992840 | HCID 56992840 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 88176874 | HCID 88176874 | — |
Reaction Steps
4N Hydrochloric acid--ethyl acetate solution (0.35 ml) was added to a solution of N-[3-(dimethylamino)propyl]-{2-[(N-octadecylcarbamoyloxy)methyl]phenyl}formamide (0.49 g) in ethyl acetate (10 ml) at room temperature. After being stirred for 5 minutes, the reaction mixture was concentrated. The residue was recrystallized from ethyl acetate, thereby yielding 0.41 g of the aimed compound as white crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06114325 |
| Source dataset | uspto-grants-2000_09 |
| ORD ID | ord-4008010ea445409c9e17abe4b1e30ebf |
| Source note | uspto-grants-2000_09 |