HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 88177255, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 54102642 | HCID 54102642 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 88177255 | HCID 88177255 | — |
Reaction Steps
4N Hydrochloric acid--ethyl acetate solution (0.20 ml) was added to a solution of [2-[[N-[2-(diethylamino)ethyl]carbamoyloxy]methyl]phenyl]-N-octadecylformamide (0.42 g) in ethyl acetate (5 ml) at room temperature. After being stirred for 15 minutes, the reaction mixture was concentrated. The residue was recrystallized from ethyl acetate-ethanol mixed solvent, thereby yielding 0.35 g of the aimed compound as white crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06114325 |
| Source dataset | uspto-grants-2000_09 |
| ORD ID | ord-7a3f3b1f031d4c9a9105c1b1ea9075f7 |
| Source note | uspto-grants-2000_09 |