HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 23299378, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 15484867 | HCID 15484867 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 23299378 | HCID 23299378 | — |
Reaction Steps
4N Hydrochloric acid--ethyl acetate solution (0.40 ml) was added to a solution of [2-(N-octadecylcarbamoyl)phenyl]methyl 4-(2-hydroxyethyl)piperazinecarboxylate (0.45 g) in ethyl acetate (10 ml) at room temperature. After being stirred for 10 minutes, the reaction mixture was concentrated. The residue was recrystallized from ethyl acetate-ethanol mixed solvent, thereby yielding 0.39 g of the aimed compound as white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06114325 |
| Source dataset | uspto-grants-2000_09 |
| ORD ID | ord-e4280b6f3958423c97366694add6ec77 |
| Source note | uspto-grants-2000_09 |