HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 70304038, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 86755726 | HCID 86755726 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 70304038 | HCID 70304038 | — |
Reaction Steps
4N Hydrochloric acid--ethyl acetate solution (1.44 ml) was added to a solution of 2-[2-(octadecylamino)-2-oxoethyl]benzyl-4methyl-1-piperazinecarboxylate (2.60 g) in ethyl acetate (39 ml) at room temperature. After being stirred for 30 minutes, the reaction mixture was concentrated. The residue was recrystallized from ethyl acetate-ethanol mixed solvent, thereby yielding 2.42 g of the aimed compound as white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06114325 |
| Source dataset | uspto-grants-2000_09 |
| ORD ID | ord-0f0f600f37504d68ac42f1a02b05cff1 |
| Source note | uspto-grants-2000_09 |