Potassium Carbonate → HCID 23299342, compound

HRID 1952820Notes

Reaction equation

HRID 1952820 reaction equation
[OH:1][CH2:2][C:3]1[CH:8]=[CH:7][CH:6]=[CH:5][C:4]=1[C:9]([N:11]([CH3:30])[CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][CH2:27][CH2:28][CH3:29])=[O:10].Br[CH2:32][CH2:33][CH2:34][CH2:35][Cl:36].C(=O)([O-])[O-].[K+].[K+]>CC(C)=O>[Cl:36][CH2:35][CH2:34][CH2:33][CH2:32][O:1][CH2:2][C:3]1[CH:8]=[CH:7][CH:6]=[CH:5][C:4]=1[C:9]([N:11]([CH3:30])[CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][CH2:27][CH2:28][CH3:29])=[O:10]

Participants

5

Reactant 3

HCID 11430Potassium CarbonateHCID 813641-Bromo-4-chlorobutaneHCID 23299352HCID 23299352, compound

Product 1

HCID 23299342HCID 23299342, compound

Reagents, catalysts & solvents 1

HCID 180AcetoneSolvent

Procedure

[2-(Hydroxymethyl)phenyl]-N-methyl-N-octadecylformamide is reacted with 1-bromo-4-chlorobutane in acetone in the presence of potassium carbonate at the reflux temperature of the solvent to obtain [2-(4-chlorobutoxymethyl)phenyl]-N-methyl-N-octadecylformamide.

Sources & evidence

ORD record
ord-e55fd26378ca4461a07f66afc093377f
Source dataset
uspto-grants-2000_09
Patent number
US06114325

Reaction notes

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