HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonium formate → HCID 9926403, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonium formate | HCID 2723923 | — |
| Reactant | HCID 10494397 | HCID 10494397 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 9926403 | HCID 9926403 | — |
Reaction Steps
1 g of the product obtained in Example 6, 1.2 g of ammonium format and 0.2 g of 10% Pd/C in 70 ml of ethanol are heated at reflux for 3 hours, then filtered and concentrated. The expected product is isolated by chromatography on silica gel (eluant: cyclohexane/ethyl acetate: 90/10).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06114360 |
| Source dataset | uspto-grants-2000_09 |
| ORD ID | ord-2ce35f2c1a7f4144be33a13d7e0a8aad |
| Source note | uspto-grants-2000_09 |