HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzeneacetic acid, 4-methoxy-alpha-(4-methoxyphenyl)- → HCID 137182955, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzeneacetic acid, 4-methoxy-alpha-(4-methoxyphenyl)- | HCID 94979 | — |
| Reactant | O-(Benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate | HCID 2733207 | — |
| Reactant | HCID 136333697 | HCID 136333697 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 137182955 | HCID 137182955 | 48% |
Reaction Steps
Prepared analogously to Example 14c) from bis-(4-methoxyphenyl)-acetic acid, (R)-N-[[4-(aminocarbonylaminomethyl)phenyl]methyl]-N5 -[amino(nitroimino)methyl]-ornithinamidehydrochloride and TBTU in a yield of 48% of theory. Colourless crystals, Mp. 149-151° C. (Acetonitrile).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06114390 |
| Source dataset | uspto-grants-2000_09 |
| ORD ID | ord-1499d3c529a34e50bb218839fab51e19 |
| Source note | uspto-grants-2000_09 |