HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 23301836, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 23301864 | HCID 23301864 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 23301836 | HCID 23301836 | 81% |
Reaction Steps
Prepared analogously to Example 43b) from 1-[(4-cyanophenyl)methyl]imidazolidin-2-one by catalytic hydrogenation using palladium/activated charcoal and in the presence of 1 equivalent of 1N hydrochloric acid in a yield of 81% of theory. Colourless crystals, Mp. >250° C. (Tetrahydrofuran).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06114390 |
| Source dataset | uspto-grants-2000_09 |
| ORD ID | ord-b6b34851cb80465d9c11a09952966d19 |
| Source note | uspto-grants-2000_09 |