HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 54357069, compound → HCID 23301812, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 54357069 | HCID 54357069 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 23301812 | HCID 23301812 | 60% |
Reaction Steps
Prepared analogously to Example 45f), but using tetrahydrofuran instead of ethanol as solvent, from phenylmethyl 1-(ethoxycarbonylmethyl)-1H-indole-3-acetate by catalytic hydrogenation in the presence of palladium/activated charcoal in a yield of 60% of theory. Colourless crystal, Mp. 138° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06114390 |
| Source dataset | uspto-grants-2000_09 |
| ORD ID | ord-3a06b595cf3e4e7c8674dd164c736fe7 |
| Source note | uspto-grants-2000_09 |