HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dichloromethane → HCID 86755815, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dichloromethane | HCID 6344 | — |
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | HCID 23301851 | HCID 23301851 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 86755815 | HCID 86755815 | 61% |
Reaction Steps
Prepared analogously to Example 61e), but using tetrahydrofuran as solvent instead of dichloromethane, from 4-[2-(aminocarbonylamino)ethyl]-N-[(1,1-dimethylethoxy)carbonyl]benzenemethanamine and trifluoroacetic acid in a yield of 61% of theory. Colourless crystals, which were used in the following step without total purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06114390 |
| Source dataset | uspto-grants-2000_09 |
| ORD ID | ord-6e8a098219884666bf1e1ed5035002a7 |
| Source note | uspto-grants-2000_09 |