HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → HCID 23301966, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | HCID 23301852 | HCID 23301852 | — |
| Catalyst | Nickel | HCID 935 | — |
| Product | HCID 23301966 | HCID 23301966 | — |
Reaction Steps
Prepared analogously to Example 6c) from 4-[[[[3-(dimethylamino)propyl]amino]carbonyl]methyl]benzonitrile by catalytic hydrogenation in the presence of Raney nickel and ammonia in a quantitative yield. Colourless, highly viscous oil, which was used in the next step without purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06114390 |
| Source dataset | uspto-grants-2000_09 |
| ORD ID | ord-e931fbe726b64770aea304a60a7a8b34 |
| Source note | uspto-grants-2000_09 |