反应详情

To a solution of (2-pyridyl)acetonitrile (12.0 g, 0.10 mole) in 150 ml of carbon tetrachloride, was added 18.1 g of N-bromosuccinimide (0.10 mole) at room temperature. The mixture was refluxed for 1.5 h. The resulting precipitate was removed by filtration and the solvent was removed under reduced pressure to give the crude product, which was recrystallized from hexane to yield 18.6 g (94%) of the title compound as red crystals:

1. temperatureThe mixture was refluxed for 1.5 h
2. customThe resulting precipitate was removed by filtration
3. customthe solvent was removed under reduced pressure
4. customto give the crude product, which
5. customwas recrystallized from hexane